Analysis of hydrogen in a hydrogenated, 3D-printed Ti–6Al–4V alloy by glow discharge optical emission spectroscopy: sample heating effects

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dc.contributor.authorWeiss, Zdeněk
dc.contributor.authorČapek, Jaroslav
dc.contributor.authorKačenka, Zdeněk
dc.contributor.authorEkrt, Ondřej
dc.contributor.authorKopeček, Jaromír
dc.contributor.authorLosertová, Monika
dc.contributor.authorVojtěch, Dalibor
dc.date.accessioned2024-10-21T08:57:59Z
dc.date.available2024-10-21T08:57:59Z
dc.date.issued2024
dc.description.abstractDepth profile analysis of a hydrogenated Ti–6Al–4V alloy by glow discharge optical emission spectroscopy (GDOES) is described. Besides the earlier reported ‘hydrogen effects’, causingchanges in emission intensities of other elements if hydrogen is present, the analysis of hydrogen itself was found to be affected by the redistri bution of hydrogen inthe region adjacent to the analyzed spot, due to sample heating and the thereby increased hydrogen diffusivity. A simple model of heat transfer within the sample during the GDOES analysis is proposed and the surface temperature of the analyzed spot is estimated to be z365 °C, in the given experimental setup.cs
dc.description.firstpage996cs
dc.description.issue4cs
dc.description.lastpage1003cs
dc.description.sourceWeb of Sciencecs
dc.description.volume39cs
dc.identifier.citationJournal of Analytical Atomic Spectrometry. 2024, vol. 39, issue 4, p. 996-1003.cs
dc.identifier.doi10.1039/d3ja00434a
dc.identifier.issn0267-9477
dc.identifier.issn1364-5544
dc.identifier.urihttp://hdl.handle.net/10084/155182
dc.identifier.wos001186373500001
dc.language.isoencs
dc.publisherRoyal Society of Chemistrycs
dc.relation.ispartofseriesJournal of Analytical Atomic Spectrometrycs
dc.relation.urihttps://doi.org/10.1039/D3JA00434Acs
dc.rightsThis journal is © The Royal Society of Chemistry 2024cs
dc.rights.accessopenAccesscs
dc.rights.urihttp://creativecommons.org/licenses/by/3.0/cs
dc.titleAnalysis of hydrogen in a hydrogenated, 3D-printed Ti–6Al–4V alloy by glow discharge optical emission spectroscopy: sample heating effectscs
dc.typearticlecs
dc.type.statusPeer-reviewedcs
dc.type.versionpublishedVersioncs

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